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6,972,107 System for direct electrowinning of copper

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US006972107B2

(12) United States Patent

Marsden et al.

(10) Patent No.:

(45) Date of Patent:

US 6,972,107 B2

Dec. 6,2005

(54) SYSTEM FOR DIRECT ELECTROWINNING

OF COPPER

(56) References Cited

U.S. PATENT DOCUMENTS

OTHER PUBLICATIONS

(75) Inventors: John O. Marsden, Phoenix, AZ (US);

Robert E. Brewer, Safford, AZ (US);

Joanna M. Robertson, Thatcher, AZ

(US); David R. Baughman, Golden,

CO (US); Philip Thompson, West

Valley City, UT (US); Wayne W.

Hazen, Lakewood, CO (US); Christel

M. A. Bemelmans, Indian Hills, CO

(US)

3,917,519 A

3,949,051 A

4,093,526 A

4,338,168 A

5,223,024 A

5,232,491 A

6,451,089 B1

6,663,689 B2 *

11/1975 Fisher et al.

4/1976 Pawlek

6/1978 Blanco et al.

7/1982 Stanley et al.

6/1993 Jones

8/1993 Corrans et al.

9/2002 Marsden et al.

12/2003 Marsden et al. .............. 75/744

(73) Assignee: Phelps Dodge Corporation, Phoenix,

AZ (US)

( *) Notice:

Prior Publication Data

ABSTRACT

14 Claims, 2 Drawing Sheets

A system and process for recovering copper from a coppercontaining

ore, concentrate, or other copper-bearing material

to produce high quality cathode copper from a leach solution

without the use of copper solvent extraction techniques or

apparatus. A process for recovering copper from a coppercontaining

ore generally includes the steps of providing a

feed stream containing comminuted copper-containing ore,

concentrate, or other copper-bearing material, leaching the

feed stream to yield a copper-containing solution, conditioning

the copper-containing solution through one or more

physical or chemical conditioning steps, and electrowinning

copper directly from the copper-containing solution, without

subjecting the copper-containing solution to solvent extraction.

PCT/US 02/23454, PCT International Search Report, dated

Jun. 20, 2003.

(57)

* cited by examiner

Primary Examiner--5cott Kastler

(74) Attorney, Agent, or Firm-Snell & Wilmer LLP

US 2004/0130076 Al Jul. 8, 2004

Filed: Dec. 15, 2003

Subject to any disclaimer, the term of this

patent is extended or adjusted under 35

U.S.c. 154(b) by 0 days.

Appl. No.: 10/737,420

Related U.S. Application Data

Continuation of application No. 10/238,399, filed on

Sep. 9, 2002, now Pat. No. 6,663,689, which is a

continuation of application No. 09/912,921, filed on

Jul. 25, 2001, now Pat. No. 6,451,089.

Int. CI? . ... ... ... ... ..... ... ... ... C22B 3/06

U.S. Cl. 266/171; 266/101; 205/367

Field of Search 266/171, 101;

75/744; 205/367

(63)

(51)

(52)

(58)

(21)

(22)

(65)

119

116

109

1010

1040

113 114

: 1051

1060

108 1070

106

- - - - --- - - ---- - -- - -- - - - - - -- - - -, 110

: 1021

1020 J :

u.s. Patent Dec. 6,2005 Sheet 1 of 2 US 6,972,107 B2

101

1GB 1010

Cu SEPARATION

109

102

- - - - - - - - - - - - - - - - -

I "\10

THICKENER

I

1 - _l

1 1021

1020/:

I

103

PRESSURE LEACHING

1030 / : - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

104

118

119

1040

FLASH

105

114

CCD

: 1051

113

1050 / : - - - - - - - - - - - - - - - - - - - - - - - - - - - - 106

1060

ELECTROLYTE RECYCLE TANK

108 1070

107

ELECTROWINNING

116

Cu

FIG. 1

u.s. Patent Dec. 6,2005 Sheet 2 of 2 US 6,972,107 B2

( SUBGRADE ORE) (EVAP.)

201

107 115

203

204 204 ---------------------_1- I

ELECTROLYTE

RECYCLE TANK

ELECTROWINNING

ELECTROWINN-ING

2020

1070

2030

208

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FIG. 2

US 6,972,107 B2

2

SUMMARY OF THE INVENTION

While the way in which the present invention addresses

the deficiencies and disadvantages of the prior art is

described in greater detail hereinbelow, in general, according

to various aspects of the present invention, a process for

25 recovering copper and other metal values from a coppercontaining

material includes obtaining a copper-containing

solution from, for example, a pressure leaching system, and

then appropriately conditioning the copper-containing solution

for electrowinning. In a preferred aspect of the inven-

30 tion, the composition of the copper-containing solution is

similar to the composition of the electrolyte produced by a

solvent extraction circuit, for example, with respect to acid

and copper concentrations. In accordance with the various

embodiments of the present invention, however, the copper-

35 containing solution is not subjected to solvent extraction.

In accordance with an exemplary embodiment of the

present invention, a process for recovering copper from a

copper-containing material generally includes the steps of:

(i) providing a feed stream containing copper-containing

40 material; (ii) subjecting the copper-containing feed stream to

atmospheric leaching or pressure leaching to yield a coppercontaining

solution; (iii) conditioning the copper-containing

solution through one or more chemical or physical conditioning

steps; and (iv) electrowinning copper directly from

45 the copper-containing solution, without subjecting the copper-

containing solution to solvent extraction. As used herein,

the term "pressure leaching" shall refer to a metal recovery

process in which material is contacted with an acidic solution

and oxygen under conditions of elevated temperature

50 and pressure.

In accordance with an exemplary embodiment of the

present invention, a process for recovering copper from a

copper-containing material generally includes the steps of:

(i) providing a feed stream containing copper-containing

55 material; (ii) subjecting the copper-containing feed stream to

atmospheric leaching or pressure leaching to yield a coppercontaining

solution; (iii) conditioning the copper-containing

solution through one or more chemical or physical conditioning

steps; and (iv) electrowinning copper directly from

60 the copper-containing solution, without subjecting the copper-

containing solution to solvent extraction. As used herein,

the term "pressure leaching" shall refer to a metal recovery

process in which material is contacted with an acidic solution

and oxygen under conditions of elevated temperature

65 and pressure.

In one aspect of a preferred embodiment of the invention,

one or more processing steps are used in order to separate

providing a concentrated copper solution suitable for electrowinning

of highly pure copper metal. Direct electrowinning

of copper-that is, plating of copper directly from the

pregnant leach solution without the intervening step of

5 purification by solvent extraction-is known. However, the

copper recovered by such so-called direct electrowinning

processes often is too impure for sale or use as is, and thus,

generally must be further refined at an additional cost, or

may be sold at a discount. More specifically, prior art

10 techniques have shown the ability for direct electrowinning

of copper to produce a relatively low-quality copper product.

An effective and efficient method to recover copper from

copper-containing materials, especially copper from copper

15 sulfides such as chalcopyrite and chalcocite, that enables

high copper recovery to be achieved at a reduced cost over

conventional processing techniques would be advantageous.

FIELD OF INVENTION

CROSS REFERENCE TO RELATED

APPLICATIONS

BACKGROUND OF THE INVENTION

1

SYSTEM FOR DIRECT ELECTROWINNING

OF COPPER

This application is a continuation of U.S. Patent application

Ser. No. 10/238,399, filed on Sep. 9, 2002, now U.S.

Pat. No. 6,663,689 which is a continuation of U.S. Patent

application Ser. No. 09/912,921, which was filed on Jul. 25,

2001 and issued as U.S. Pat. No. 6,451,089 on Sep. 17,2002,

the disclosures of which are incorporated by reference

herein.

Hydrometallurgical treatment of copper containing materials,

such as copper ores, concentrates, and other copperbearing

materials, has been well established for many years.

Currently, there exist many creative approaches to the

hydrometallurgical treatment of these materials; however,

common to almost all of the processes either now known or

under development is the use of solvent extraction and

electrowinning (SX-EW) for solution purification and copper

recovery. Although SX-EW is not without its drawbacks,

the proven success in the copper SX-EW field has made this

approach standard for production of high quality copper

products.

The traditional hydrometallurgical process for copper

recovery involves first leaching copper-containing material

with an acidic solution, either atmospherically or under

conditions of elevated temperature and pressure. The resultant

process stream-the so-called pregnant leach

solution-is recovered, and in a solvent extraction (or solution

extraction, as it is sometimes called) stage, is mixed

with an organic solvent (i.e., an extractant), which selectively

removes the copper from the pregnant leach solution.

The copper-loaded extractant is then mixed with an aqueous

acid solution, which strips the copper from the extractant,

producing a solution stream suitable for electrowinning.

This resultant solution stream is highly concentrated and

relatively pure, and typically is processed into high quality

copper cathode in an electrowinning circuit.

In general, electrowinning of copper consists of the electrolytic

deposition (sometimes called "plating") of copper

onto a cathode and the evolution of oxygen at an anode. In

a simple design of an exemplary electrowinning unit, a set

of cathodes and anodes are set in a reaction chamber

containing the copper-containing electrolyte. When the unit

is energized, copper ions are reduced onto the cathode (i.e.,

plated). Plating of copper typically occurs on copper starter

sheets or stainless steel blanks. Anodes are quasi-inert in the

electrolyte and provide a surface for oxygen evolution. The

copper plates produced by the electrowinning unit can be in

excess of 99.99 percent pure.

Purification of copper from the pregnant leach solution by

solvent extraction has proven to be a successful means of

The present invention relates generally to a process for

recovering copper from a copper-containing ore, concentrate,

or other copper-bearing material, and more specifically,

to a process for producing cathode copper without the 20

use of solvent/solution extraction, ion exchange of copper,

or related processes to refine and concentrate the copperbearing

solution.

3

US 6,972,107 B2

4

copper from the acid in a recycled portion of the lean

electrolyte from the direct electrowinning process, thus

enabling the rejection of a portion of the acid component

from the process circuit without rejecting a significant

portion the copper. As discussed in greater detail hereinbelow,

a number of conventional or hereafter devised processes

may be utilized to separate copper from acid in the

feed stream. For example, in accordance with one aspect of

an exemplary embodiment of the invention, a copper precipitation

step may be utilized to precipitate solubilized

copper from a lean electrolyte stream onto the surfaces of

solid particles in a copper-containing material stream in

advance of the pressure leaching step, thus separating the

copper from the acid solution.

In an aspect of another embodiment of the invention, a

recycle circuit is used intermediate to the leaching and

electrowinning steps to facilitate control of the composition

of copper-containing solution entering the electrowinning

stage, and to thus enhance the quality of the copper recovered

therefrom.

In accordance with various preferred aspects of the

present invention, by providing for the electrowinning of

copper directly from a copper-containing solution without

first subjecting the copper-containing solution to solvent

extraction, the present invention enables lower-cost recovery

of copper and eliminates the expenses associated with

solvent extraction, such as specialized reagents, process

apparatus and equipment, and energy resources. Furthermore,

in accordance with one preferred aspect of the invention,

careful control of the composition of the coppercontaining

solution entering the electrowinning circuit

enables production of high quality, uniformly-plated cathode

copper.

These and other advantages of a process according to

various aspects of the present invention will be apparent to

those skilled in the art upon reading and understanding the

following detailed description with reference to the accompanying

figures.

BRIEF DESCRIPTION OF THE DRAWINGS

The subject matter of the present invention is particularly

pointed out and distinctly claimed in the concluding portion

of the specification. A more complete understanding of the

present invention, however, may best be obtained by referring

to the detailed description and claims when considered

in connection with the drawing figures, wherein like numerals

denote like elements and wherein:

FIG. 1 illustrates a flow diagram of a copper recovery

process in accordance with an exemplary embodiment of the

present invention; and

FIG. 2 illustrates a flow diagram of a copper recovery

process in accordance with an alternative embodiment of the

present invention.

DETAILED DESCRIPTION OF EXEMPLARY

EMBODIMENTS

The present invention exhibits significant advancements

over prior art processes, especially other so-called "direct

electrowinning" processes, particularly with regard to product

quality and process efficiency. Moreover, existing copper

recovery processes that utilize a conventional atmospheric

or pressure leaching/solvent extraction/electrowinning process

sequence may, in many instances, be easily retrofitted

to exploit the many commercial benefits the present invention

provides.

In one aspect of a preferred embodiment of the invention,

the relatively large amount of acid generated during the

electrowinning stage as a copper-containing electrolyte

stream is transported out of the copper recovery process

5 after a separation step in which substantially all of the

copper is removed from the acid stream. It is generally

economically advantageous to utilize this generated acid

stream in some way, rather than to neutralize or dispose of

it. Thus, as discussed in greater detail hereinbelow, the

10 present invention may find particular utility in combination

with conventional atmospheric leaching operations, such as,

for example, heap leaching, vat leaching, dump or stockpile

leaching, pad leaching, agitated tank leaching, and bacterial

leaching operations, which often require a substantially

15 continuous acid supply.

In one aspect of an exemplary embodiment of the present

invention, a feed stream containing copper-containing material

is provided for processing. In accordance with the

various embodiments of present invention, the copper-con-

20 taining material may be an ore, a concentrate, or any other

copper-bearing material from which copper and/or other

metal values may be recovered. The copper in the coppercontaining

material may be in the form of copper oxides,

copper sulfides or other copper minerals, and the copper-

25 containing material may include any number of a variety of

other metals, such as, for example, gold, platinum group

metals, silver, zinc, nickel, cobalt, molybdenum, rare earth

metals, rhenium, uranium and mixtures thereof. Various

aspects and embodiments of the present invention prove

30 especially advantageous in connection with the recovery of

copper from copper sulfide ores, such as, for example,

chalcopyrite (CuFeS2 ), chalcocite (Cu2 S), bornite

(CusFeS4), and covellite (CuS).

The feed stream of copper-containing material can be

35 provided in any number of ways, such that the conditions of

the feed stream are suitable for the chosen processing

methods. For example, feed stream conditions such as

particle size, composition, and component concentrations

can affect the overall effectiveness and efficiency of down-

40 stream processing operations, such as, for example, atmospheric

leaching or pressure leaching.

In accordance with a preferred aspect of the invention, the

particle size of the copper-containing feed material is

reduced to facilitate fluid transport and to optimize the

45 processing steps of atmospheric or pressure leaching and

subsequent metal recovery processes. A variety of acceptable

techniques and devices for reducing the particle size of

the copper-containing material are currently available, such

as ball mills, tower mills, ultrafine grinding mills, attrition

50 mills, stirred mills, horizontal mills and the like, and additional

techniques may later be developed that may achieve

the desired result of increasing the surface area of the

material to be processed. With regard to one aspect of a

preferred embodiment of the invention, such a result is

55 desired because the reaction rate during leaching generally

increases as the surface area of the copper-containing material

increases, such that increasing the fineness of the copper-

containing material before subjecting the material

stream to pressure leaching generally will allow for more

60 moderate temperature and pressure conditions to be

employed within the pressure leaching vessel, and may

reduce the residence time of the oxidation reaction during

pressure leaching.

FIG. 1 illustrates an exemplary embodiment of the present

65 invention wherein copper is the metal to be recovered from

a copper-containing material, such as a sulfide ore. In

preparation for froth flotation, the copper-containing mateUS

6,972,107 B2

5 6

CuFeS2+Cu+2~Fe+2+2CuS (possible side reaction)

Other copper minerals and other sulfides react to varying

degrees according to similar reactions, producing copper

Moreover, utilization of a separation process in accordance

with this aspect of the invention may be particularly advantageous

in that it may enable contaminants from the unrefined

copper-containing material stream to be removed from

5 the copper-containing material stream and incorporated into

the resultant acid stream. Because the resultant acid stream

is preferably removed from the metal recovery process

altogether and utilized in remote operations, disposed of, or

neutralized, the contaminants contained therein are likewise

10 removed from the metal recovery process and are thus

prevented from accumulating in the process stream. This

may be a significant advantage in that such contaminants,

particularly metal contaminants, typically have a deleterious

effect on the effectiveness and efficiency of the desired metal

15 recovery process. For example, metal contaminants and

other impurities in the process stream, if not carefully

controlled and/or minimized, can contribute to diminished

physical and/or chemical properties in the cathode copper

produced by electrowinning, and can thus degrade the

20 copper product and diminish its economic value.

Referring again to FIG. 1, in accordance with one aspect

of a preferred embodiment of the invention, copper-containing

material stream 101 is subjected to a separation, such as,

for example, a precipitation step, which, in this exemplary

25 process, serves to precipitate solubilized copper from a

recycled lean electrolyte stream onto the surfaces of solid

particles in the copper-containing material stream. As discussed

in detail above, this aspect offers an important

advantage in that it enables recovery of copper from a lean

30 electrolyte stream that otherwise may have been lost or

would have required additional processing to recover, potentially

resulting in significant economic benefits.

In this preferred aspect of the invention, the precipitation

step involves the copper-containing material stream being

35 combined with a sulfur dioxide (S02) stream 109 and a lean

electrolyte stream 108 in a suitable processing vessel. For

example, in the embodiment illustrated in FIG. 1, lean

electrolyte stream 108 may comprise a recycled acidic

copper sulfate stream generated during an electrowinning

40 operation. Other streams, however, preferably copper-rich

streams, may also be used. In one aspect of this embodiment

of the invention, lean electrolyte stream 108 has an acid

concentration of from about 20 to about 200 gramslliter,

preferably from about 30 to about 150 gramslliter, and most

45 preferably from about 50 to about 120 gramslliter. In a

further aspect of this embodiment of the invention, lean

electrolyte stream 108 has a copper concentration of from

about 20 to about 55 grams/liter, preferably from about 25

to about 50 gramslliter, and most preferably from about 30

50 to about 45 gramslliter. In copper precipitation stage 1010,

copper from lean electrolyte stream 108 precipitates to form

a desired copper-rich concentrate. Preferably, precipitation

is carried out such that the copper from the lean electrolyte

precipitates, at least in part, onto the surface of unreacted

55 copper-containing material particles within stream 101 in

the form of copper sulfides, such as, for example, eus.

While not wishing to be bound by any particular theory, the

chemical reaction during this exemplary copper precipitation

step-wherein, for example, the copper-containing

60 material is primarily chalcopyrite-is believed to be as

follows:

rial feed stream is ground to a particle size suitable to

liberate mineral-bearing particles from gangue materials. In

one aspect of a preferred embodiment, copper-containing

material is comminuted using, for example, a ball mill, and

subjected to conventional flotation techniques and practices.

In one aspect of the present invention, the copper-containing

material has a PSO of less than about 250 microns, preferably

a PSO from about 75 to about 150 microns, with the optimal

size depending on flotation and liberation characteristics.

The product from flotation preferably has a PSO of less than

about 150 microns, and more preferably a PSO on the order

of from about 5 to about 75 microns. Other particle sizes and

distributions that facilitate fluid transport and subsequent

processing may, however, be utilized.

In another aspect of a preferred embodiment of the

present invention, the comminuted copper-containing material

is combined with a liquid to form a copper-containing

material stream 101. Preferably, the liquid comprises water,

but any suitable liquid may be employed, such as, for

example, raffinate, pregnant leach solution, or lean electrolyte.

For example, a portion of lean electrolyte stream 108

from the direct electrowinning process may be combined

with comminuted copper-containing material to form copper-

containing material stream 101 (not shown in FIG. 1).

In another aspect of a preferred embodiment of the

present invention, the comminuted copper-containing material

is combined with a liquid to form a copper-containing

material stream 101. Preferably, the liquid comprises water,

but any suitable liquid may be employed, such as, for

example, raffinate, pregnant leach solution, or lean electrolyte.

For example, a portion of lean electrolyte stream 108

from the direct electrowinning process may be combined

with comminuted copper-containing material to form copper-

containing material stream 101 (not shown in FIG. 1)

The combination of the liquid with the copper-containing

material can be accomplished using anyone or more of a

variety of techniques and apparatus, such as, for example,

in-line blending or using a mixing tank or other suitable

vessel. In accordance with a preferred aspect of this embodiment,

the material stream is concentrated with the coppercontaining

material being on the order less than about 50

percent by weight of the stream, and preferably about 40

percent by weight of the stream. Other concentrations that

are suitable for transport and subsequent processing may,

however, be used.

In accordance with one aspect of the present invention, it

is desirable to separate the copper in a recycled stream of

lean electrolyte from electrowinning from the acid, and also

to reduce the amount of contaminants in the portion of the

stream to be subjected to the metal recovery process. In such

a separation process, the acid that is removed from the

recycled lean electrolyte stream may be rejected from the

process circuit, taking with it at least a portion of the metal

contaminants and other soluble impurities from the coppercontaining

feed stream and the recycled lean electrolyte

stream. Any number of conventional or hereafter devised

separation processes and techniques may be useful to

achieve the separation of copper from acid in the feed

stream. For example, separation processes and/or techniques

such as precipitation, low temperature pressure leaching,

acid solvent extraction/ion exchange, membrane separation,

cementation, pressure reduction, sulfiding, and/or the use of

liberator cells may be useful for this purpose.

The separation aspect of a preferred embodiment of the

invention contributes to providing a resultant acid stream 65

that contains a relatively small fraction of copper, which can

be used for leaching, pH control, or other applications.

US 6,972,107 B2

7 8

Process effluent acid stream 110 may be utilized, processed,

neutralized, impounded, and/or disposed of in a

variety of ways, the appropriate choice of which is largely

dependent upon economic and regulatory factors. In one

5 aspect of the illustrated embodiment, the acid stream can be

beneficially used in, for example, an atmospheric leaching

operation, where acid is required to leach copper oxide or

sulfide minerals. Such a leaching operation may be a heap

leach, a vat leach, a tank leach, a pad leach, or any other

10 similar operation. Acid is consumed in these operations

through reaction with acid-consuming constituents in the

ore.

In FIG. 2, acid stream 110 from thickener circuit 1021

(FIG. 1) is sent to a conventional atmospheric leach opera-

15 tion 2010. In accordance with one aspect of a preferred

embodiment of the invention, atmospheric leach operation

2010 is a conventional acid-consuming heap leach operation,

wherein a subgrade ore 201 is contacted with acid

stream 110 and, optionally, other process streams, such as

20 raffinate stream 206 from downstream solvent extraction

unit 2020. In heap leach operation 2010, the acid percolates

downward through the ore heap, solubilizing the copper in

the copper-containing ore in the form of copper sulfate, to

form a copper-rich pregnant leach solution (PLS) stream

25 203. In conventional atmospheric leach operations, PLS

stream 203 is sent to a solvent extraction unit, such as

solvent extraction unit 2020 in FIG. 2, to produce a high

concentration and relatively pure copper sulfate solution

suitable for electrowinning. In accordance with an alterna-

30 tive aspect of the present invention illustrated in FIG. 2, PLS

stream 203 may not be subjected to solvent extraction, but

may instead be blended with other copper-containing process

streams, and the resultant stream then sent to an

electrowinning circuit. For example, all or a portion of PLS

35 stream 203 (broken line) may be blended with coppercontaining

solution stream 106 and lean electrolyte stream

115 in electrolyte recycle tank 1060 (from FIG. 1) to form

a resultant product stream suitable for electrowinning in an

electrowinning circuit.

In accordance with a further aspect of this embodiment of

the present invention, as previously briefly mentioned, acid

stream 110 advantageously may remove impurities from the

process, for example the electrowinning process. Such

impurities include, without limitation, iron, aluminum, mag-

45 nesium, sodium, potassium and the like, often present as

sulfates. In the absence of removal, such impurities may

accumulate to deleterious levels, and, as such negatively

impact production efficiencies and product (e.g. copper

cathode) quality. The presence of such impurities in acid

50 stream 110 generally does not negatively impact the aforementioned

handling of acid stream 110.

In accordance with one aspect of a preferred embodiment

of the invention illustrated in FIG. 2, solvent extraction unit

2020 purifies copper-bearing PLS stream 203 from the heap

55 leach in two unit operations-an extraction operation, which

may have multiple stages, followed by a stripping operation.

In the extraction stage, PLS stream 203 is contacted with an

organic phase consisting of a diluent in which a copper

selective reagent (i.e., the extractant) is dissolved. When the

60 solutions are contacted, the organic extractant chemically

removes the copper from the PLS, forming an aqueous

raffinate stream. The raffinate and organic streams are subsequently

separated in a settler. After separation of the

organic and aqueous phases in the settler, a portion of the

65 aqueous phase (stream 206) is typically returned to one or

more leaching operations to be reloaded with copper from

the ore in the atmospheric leach to form the PLS. The

precipitates and a weak sulfuric acid by-product. In accordance

with a preferred aspect of the invention, copper

separation stage 1010 is carried out at a slightly elevated

temperature, such as from about 70° C. to about 180° c.,

preferably from about 80° C. to about 100° c., and most

preferably at a temperature of about 90° C. Heating, if

necessary, can be effectuated through any conventional

means, such as electric heating coils, a heat blanket, process

fluid heat exchange, and other ways now known or later

developed. In the exemplary process of FIG. 1, steam

generated in other process areas, such as stream 119 from

flash tank 1040 or stream 118 from pressure leaching stage

1030, may be directed to the processing vessel in copper

separation stage 1010 to provide the heat desired to enhance

the precipitation process. The residence time for the copper

precipitation process can vary, depending on factors such as

the operating temperature of the processing vessel and the

composition of the copper-containing material, but typically

ranges from about thirty (30) minutes to about 6 hours.

Preferably, conditions are selected such that significant

amounts of copper are precipitated. For example, precipitation

rates on the order of about 98% precipitation of copper

have been achieved in processing vessels maintained at

about 90° C. for about 4 hours.

Other parameters to consider when conditioning the copper-

containing material feed stream for processing are the

fraction of solid particles in the feed stream and the total

volume of the feed stream. Thus, these or other parameters,

such as, for example, temperature, pressure, viscosity, density,

composition, and the like, may be suitably addressed.

Although these parameters mayor may not be significant to

the overall efficiency of processing operations downstream

in all cases, these parameters can affect equipment size and

material specifications, energy requirements, and other

important aspects of process design. Thus, calculated adjustment

of these stream parameters in advance of complex or

resource-intensive processing stages can positively affect

the economic efficiency of the chosen process. Solid-liquid

separation systems, such as, for example, filtration systems,

counter-current decantation (CCD) circuits, thickeners, and 40

the like are useful in adjusting these parameters and are

widely used in the industry.

In one aspect of the embodiment of the invention illustrated

in FIG. 1, product stream 102, which generally

contains covellite/chalcopyrite particles and acid, contains a

large fraction of acid generated in pressure leaching stage

1030 and electrowinning stage 1070, and the acid generated

in copper separation stage 1010.

In accordance with a preferred aspect of the invention, the

copper-containing material stream entering the pressure

leaching stage contains from about 10 to about 50 percent

solids by weight, preferably from about 20 to about 40

percent solids by weight. To adjust the solids concentration

of product stream 102 in accordance with the desired

parameters, in accordance with an exemplary embodiment

of the invention, product stream 102 is sent to a solid-liquid

separation circuit 1020. In one aspect of a preferred embodiment

of the invention, solid-liquid separation circuit 1020

preferably includes a wash thickener circuit 1021 comprising

multiple thickener stages arranged in a counter-current

decantation (CCD) configuration that effectuate separation

of a substantial amount of the acid in the product stream

from the copper-containing solid particles therein. In the

illustrated embodiment, the underflow of thickener circuit

1021 is pressure leaching feed stream 103 and the overflow

is acid stream 110. Preferably, acid stream 110 contains only

a negligible amount of copper.

US 6,972,107 B2

9 10

4CuFeS2+4H2S04+502~4CuS04+2Fe203+8S0+4H20

2CuS+2H2S04+02~2Cu+2+2S04-2+2H20+2So

If desired, conditions during pressure leaching can be

controlled such that a portion of the sulfide sulfur contained

in the feed stream is converted to elemental sulfur instead of

sulfate. The fraction of chalcopyrite and covellite that form

sulfur instead of sulfate are believed to react according to the

following equations:

Pressure leaching, for example in pressure leaching vessel

1031, preferably occurs in a manner suitably selected to

promote the solubilization of copper using these (or other)

processes. In general, temperature and pressure in the pressure

leaching vessel should be carefully controlled. For

example, in accordance with one aspect of the invention, the

temperature of pressure leaching vessel 1031 is maintained

at from about 100° C. to about 250° c., preferably from

about 140° C. to about 235° C. In accordance with one

aspect of one embodiment of the invention, the temperature

of pressure leaching vessel 1031 is advantageously maintained

at from about 140° C. to about 180° C. or in the range

of from about 150° C. to about 175° C. In accordance with

another embodiment of the invention, the temperature of

pressure leaching vessel 1031 is advantageously maintained

between from about 200° C. to about 235° C. or in the range

of from about 210° C. to about 225° C. Furthermore, the

total operating pressure in pressure leaching vessel 1031 is

necessarily superatmospheric, ranging from about 50 to

about 750 psi. In accordance with one aspect of one embodiment

of the invention, the pressure is advantageously in the

range of between from about 200 to about 450 psi, and more

preferably from about 250 to about 400 psi. In accordance

with another embodiment of the invention, the pressure is

advantageously maintained between from about 400 or

about 500 to about 700 psi.

During pressure leaching, it is generally desirable to inject

oxygen into the pressure leaching vessel. In one aspect of a

preferred embodiment of the invention, during pressure

leaching in pressure leaching vessel 1031, sufficient oxygen

112 is injected into the vessel to maintain an oxygen partial

pressure in pressure leaching vessel 1031 of from about 50

to about 200 psi, preferably from about 75 to about 150 psi,

and most preferably from about 100 to about 125 psi.

Because pressure leaching of many metal sulfides is a

highly exothermic process and the heat generated is generally

greater than that required to heat pressure leaching feed

stream 103 to the desired operating temperature, cooling

liquid 111 is preferably contacted with pressure leaching

feed stream 103 in pressure leaching vessel 1031 during

pressure leaching. Cooling liquid 111 is preferably process

water, but can be any suitable cooling fluid from within the

refining process or from an outside source. In a preferred

components at the desired temperature and pressure conditions

for the requisite processing residence time. In a preferred

embodiment, a pressure leaching vessel 1031 is

employed for this purpose. Pressure leaching vessel 1031 is

5 preferably a multi-compartment, agitated vessel.

Generally, the chemical conversions that occur during

pressure leaching stage 1030 under certain conditions for the

solubilization of the copper in copper-containing materials,

such as chalcopyrite, chalcocite, or covellite are as follows:

organic stream passes on to the second unit operation of the

solvent extraction process, the stripping operation. In the

stripping operation, the organic stream is contacted with a

strongly acidic electrolyte. This acidic solution "strips" the

copper from the extractant, leaving the organic phase substantially

depleted of copper. At least a portion of the loaded

strip solution aqueous phase (stream 204) is advanced to an

electrowinning plant 2030 as a copper "rich" solution.

Aqueous stream 204 is processed in electrowinning plant

2030 to yield cathode copper 207 and a copper-containing 10

lean electrolyte stream 208, which, in one aspect of a

preferred embodiment of the invention, may be recycled in

part to solvent extraction unit 2020.

In accordance with one alternative aspect of the invention,

aqueous stream 204 may not be subjected to electrowinning 15

immediately after leaving the solvent extraction unit, but

may instead be blended with other copper-containing process

streams, and the resultant stream then sent to an

electrowinning circuit. For example, all or a portion of

aqueous stream 204 (broken line) may be blended with 20

copper-containing solution stream 106 and lean electrolyte

stream 115 in electrolyte recycle tank 1060 (from FIG. 1) to

form a resultant product stream suitable for electrowinning

in an electrowinning circuit 1070. In such cases the stripping

solutions used in solvent extraction 2020 likely will be 25

comprised of spent electrolyte from electrowinning circuit

1070.

If effluent acid stream 110 is not used as a by-product

reagent or otherwise utilized, the acid may be neutralized

using, for example, acid-consuming gangue (i.e., mineral 30

processing tailings) or a neutralizing agent, such as limestone

or lime. Neutralizing with acid-consuming gangue can

be relatively inexpensive, as the neutralizing reagent is

essentially free. On the other hand, neutralizing with limestone

or lime may be less desirable economically, as both 35

these reagents will incur cost. Nevertheless, should neutralization

be desired, any method for acid neutralization now

known or hereafter devised may be employed.

Referring again to FIG. 1, the underflow slurry from wash

thickener circuit 1021, pressure leaching feed stream 103 in 40

this preferred embodiment of the invention, has a composition

of about 40 to about 60 percent solids by weight, the

balance being a dilute acid solution. The general composition

of the dilute acid solution is dependent upon the ratio of

process water to acid introduced in the thickener circuit (i.e., 45

the wash ratio).

In a further aspect of the present invention, the conditioned

copper-containing feed stream preferably is subjected

to a suitable process, such as pressure leaching, to produce

a product slurry 104, which comprises a copper-containing 50

solution and a residue 114. The process may be selected as

desired, but, in general, enables production of a coppercontaining

solution that exhibits copper and acid concentrations

similar to an electrolyte stream resulting from a solvent

extraction circuit-that is, the copper-containing solution 55

preferably is suitable for processing in an electrowinning

circuit. Any suitable technique or combination of techniques

that yields an appropriate copper-containing solution without

employing solvent-extraction techniques may be used.

In a preferred embodiment of the invention, as illustrated in 60

FIG. 1, pressure leaching feed stream 103 is subjected to a

pressure leaching stage 1030 to yield a copper-containing

product slurry 104.

In accordance with one aspect of this embodiment of the

present invention, pressure leaching feed stream 103 is 65

transported to a suitable vessel for pressure leaching, which

can be any vessel suitably designed contain the process

11

US 6,972,107 B2

12

embodiment of the invention, a sufficient amount of cooling

liquid 111 is added to pressure leaching vessel 1031 to yield

a solids content in the product slurry 104 ranging from about

3 to about 15 percent solids by weight.

The residence time for pressure leaching generally

depends on a number of factors, including the composition

of the copper-containing feed stream and the operating

pressure and temperature of the pressure leaching vessel. In

one aspect of the invention, the residence time for pressure

leaching ranges from about thirty minutes to about three

hours.

In another aspect of the present invention, the coppercontaining

solution is conditioned for electrowinning

through one or more chemical and/or physical processing

steps. In much the same way that the copper-containing

material feed stream is conditioned for processing in accordance

with above-described aspects of the invention, the

copper-containing solution intended to be utilized in the

electrowinning circuit of the present invention is conditioned

to adjust the composition, component concentrations,

volume, temperature, and/or other physical and/or chemical

parameters to desired values. Generally, a properly conditioned

copper-containing solution will contain a relatively

high concentration of copper in an acid solution and will

contain few impurities. Preferably, the conditions of coppercontaining

solution entering the electrowinning circuit are

kept at a constant level to enhance the quality and uniformity

of the cathode copper product.

In a preferred aspect of the invention, conditioning of a

copper-containing solution for electrowinning begins by

adjusting certain physical parameters of the product slurry

from the previous processing step. In a preferred embodiment

of the invention wherein the previous processing step

is pressure leaching, it is desirable to reduce the temperature

and pressure of the product slurry. A preferred method of so

adjusting the temperature and pressure characteristics of the

preferred product slurry is atmospheric flashing.

Thus, in accordance with a preferred aspect of the

embodiment illustrated in FIG. 1, product slurry 104 from

pressure leaching vessel 1031 is flashed in an atmospheric

flash tank 1040 or other suitable atmospheric system to

release pressure and to evaporatively cool the product slurry

104 through the release of steam to form a flashed product

slurry 105. Flashed product slurry 105 preferably has a

temperature ranging from about 90° C. to about 101°C., a

copper concentration of from about 40 to about 75 grams/

liter, and an acid concentration of from about 20 to about

100 gramslliter. In one aspect of the invention, however,

flashed product slurry 105 also contains a particulate solid

residue containing, for example, the iron oxide by-product

of pressure leaching, other by-products, precious metals and

other components that are undesirable for a feed stream to an

electrowinning circuit. Thus, in accordance with the same

principles discussed above, it is desirable to subject the

flashed product slurry to a solid-liquid separation process,

such that the liquid portion of the slurry-the desired

copper-containing solution-is separated from the solid

portion of the slurry-the undesired residue.

Referring again to FIG. 1, in the illustrated embodiment

of the invention flashed product slurry 105 is directed to a

solid-liquid separation stage 1050, such as a CCD circuit

1051. In an alternative embodiment of the invention, solidliquid

separation stage 1050 may comprise, for example, a

thickener or a filter. A variety of factors, such as the process

material balance, environmental regulations, residue composition,

economic considerations, and the like, may affect

the decision whether to employ a CCD circuit, a thickener,

a filter, or other suitable device in solid-liquid separation

stage 1050. In one aspect of a preferred embodiment of the

invention, CCD circuit 1051 uses conventional countercurrent

washing of the residue stream with wash water 113 to

5 recover leached copper to the copper-containing solution

product and to minimize the amount of soluble copper

advancing to either precious metal recovery processes or

residue disposal. Preferably, large wash ratios are utilized to

enhance the effectiveness of solid-liquid separation stage

10 1050-that is, relatively large amounts of wash water 113

are added to the residue in CCD circuit 1051. Preferably, the

solution portion of the residue slurry stream is diluted by

wash water 113 in CCD circuit 1051 to a copper concentration

of from about 5 to about 200 parts per million (ppm)

15 in the solution portion of residue stream 114.

Depending on its composition, residue stream 114 from

liquid/solid separation stage 1050 may be impounded, disposed

of, or subjected to further processing, such as, for

example, precious metal recovery. For example, if residue

20 stream 114 contains economically significant amounts of

gold, silver, and/or other precious metals, it may be desirable

to recover this gold fraction through a cyanidation process or

other suitable recovery process. If gold or other precious

metals are to be recovered from residue stream 114 by

25 cyanidation techniques, the content of contaminants in the

stream, such as elemental sulfur, amorphous iron precipitates,

and unreacted copper minerals, is preferably minimized.

Such materials may promote high reagent consumption

in the cyanidation process and thus increase the expense

30 of the precious metal recovery operation. As mentioned

above, it is therefore preferable to use a large amount of

wash water or other diluent during the solid-liquid separation

process to maintain low copper and acid levels in the

solids-containing residue stream in an attempt to optimize

35 the conditions for subsequent precious metal recovery.

As previously noted, careful control of the conditions of

a copper-containing solution entering an electrowinning

circuit---especially maintenance of a substantially constant

copper composition-can enhance the quality of the elec-

40 trowon copper by, among other things, enabling even plating

of copper on the cathode and avoidance of surface porosity

in the cathode copper, which degrades the copper product

and thus may diminish its economic value. In accordance

with this aspect of the invention, such process control can be

45 accomplished using any of a variety of techniques and

equipment configurations, so long as the chosen system

and/or method maintains a sufficiently constant feed stream

to the electrowinning circuit.

Referring again to FIG. 1, in a preferred aspect of the

50 invention, copper-containing solution stream 106 from

solid-liquid separation stage 1050 is sent to an electrolyte

recycle tank 1060. Electrolyte recycle tank 1060 suitably

facilitates process control for electrowinning circuit 1070, as

will be discussed in greater detail below. Copper-containing

55 solution stream 106, which generally contains from about 40

to about 70 gramslliter of copper and from about 15 to about

100 grams/liter acid, is preferably blended with a lean

electrolyte stream 115 in electrolyte recycle tank 1060 at a

ratio suitable to yield a product stream 107, the conditions

60 of which may be chosen to optimize the resultant product of

electrowinning circuit 1070.

Referring briefly to an alternative embodiment of the

invention illustrated in FIG. 2, an additional lean electrolyte

stream 205 may be blended with lean electrolyte stream 115

65 and copper-containing solution stream 106 in electrolyte

recycle tank 1060 to produce product stream 107 in accordance

with the process control principles discussed in conUS

6,972,107 B2

13 14

65

60

recycle tank 1060 to an electrowinning circuit 1070, which

contains one or more conventional electrowinning cells.

In accordance with a preferred aspect of the invention,

electrowinning circuit 1070 yields a cathode copper product

5 116, optionally, an offgas stream 117, and a relatively large

volume of copper-containing acid, herein designated as lean

electrolyte streams 108 and 115. As discussed above, in the

illustrated embodiment of the invention, lean electrolyte

streams 108 and 115 are directed to copper precipitation

10 stage 1010 and electrolyte recycle tank 1060, respectively.

Lean electrolyte streams 108 and 115 generally have a lower

copper concentration than product stream 107, but typically

have a copper concentration of less than about 40 grams/

liter.

The present invention has been described above with

reference to a number of exemplary embodiments. It should

be appreciated that the particular embodiments shown and

described herein are illustrative of the invention and its best

mode and are not intended to limit in any way the scope of

20 the invention as set forth in the claims. Those skilled in the

art having read this disclosure will recognize that changes

and modifications may be made to the exemplary embodiments

without departing from the scope of the present

invention. For example, although reference has been made

25 throughout to copper, it is intended that the invention also be

applicable to the recovery of other metals from metalcontaining

materials. Further, although certain preferred

aspects of the invention, such as techniques and apparatus

for conditioning process streams and for precipitation of

30 copper, for example, are described herein in terms of exemplary

embodiments, such aspects of the invention may be

achieved through any number of suitable means now known

or hereafter devised. Accordingly, these and other changes

or modifications are intended to be included within the scope

35 of the present invention, as expressed in the following

claims.

What is claimed is:

1. A system for recovering copper from a copper-containing

material comprising:

a reactor, wherein said reactor is suitable for reacting at

least a portion of a copper-containing feed stream with

at least a portion of a copper-containing lean electrolyte

stream in an acidic environment to yield a pressure

leaching feed stream comprising a solid copper-bearing

precipitate and acid;

a pressure leaching vessel, wherein said pressure leaching

vessel is suitable for leaching at least a portion of said

pressure leaching feed stream in an oxidizing environment

at an elevated temperature and pressure to yield a

product slurry comprising a copper-containing solution

and a residue;

means for conditioning said product slurry without the use

of solvent extraction techniques to yield a coppercontaining

solution suitable for electrowinning and a

residue, wherein said conditioning means comprises

means for blending at least a portion of said coppercontaining

solution with at least a portion of one or

more copper-containing streams to achieve a desired

copper concentration in said copper-containing solution

suitable for electrowinning;

an electrowinning circuit, wherein said electrowinning

circuit is suitable for electrowinning copper from said

copper-containing solution to yield cathode copper and

a copper-containing lean electrolyte stream; and

means for recycling at least a portion of said coppercontaining

lean electrolyte stream from said electrowinning

circuit to said conditioning means.

Cathode half-reaction: eu2++2e---""CUO

Turning again to FIG. 1, in a preferred embodiment the

invention, product stream 107 is directed from electrolyte

nection with the embodiment illustrated in FIG. 1. In one

aspect of this alternative embodiment, lean electrolyte

stream 205 preferably has a composition similar to that of

lean electrolyte stream 115. Further, as discussed above,

other streams may be introduced to electrolyte recycle tank

1060 for blending, such as, for example, PLS stream 203

(FIG. 2).

Referring again to FIG. 1, preferably, the copper composition

of product stream 107 is maintained substantially

constant. While product stream 107 may contain a copper

concentration up to the copper solubility level under the

prevailing conditions, preferably product stream 107 has a

copper concentration of about 20 to about 80 grams/liter, and

more preferably of about 30 to about 60 gramslliter, and

often above 40 gramslliter. In one aspect of an exemplary 15

embodiment of the invention, control valves are positioned

on each of the pipelines feeding lean electrolyte stream 115

and copper-containing solution stream 106 to electrolyte

recycle tank 1060 to facilitate blending control within the

tank.

With reference to FIG. 1, copper from the product stream

107 is suitably electrowon to yield a pure, cathode copper

product. In accordance with the various aspects of the

invention, a process is provided wherein, upon proper conditioning

of a copper-containing solution, a high quality,

uniformly-plated cathode copper product 116 may be realized

without subjecting the copper-containing solution to a

solvent extraction process prior to entering the electrowinning

circuit.

As those skilled in the art are aware, a variety of methods

and apparatus are available for the electrowinning of copper

and other metal values, any of which may be suitable for use

in accordance with the present invention, provided the

requisite process parameters for the chosen method or

apparatus are satisfied. For the sake of convenience and a

broad understanding of the present invention, an electrowinning

circuit useful in connection with various embodiments

of the invention may comprise an electrowinning

circuit, constructed and configured to operate in a conven- 40

tional manner. The electrowinning circuit may include electrowinning

cells constructed as elongated rectangular tanks

containing suspended parallel flat cathodes of copper alternating

with flat anodes of lead alloy, arranged perpendicular

to the long axis of the tank. A copper-bearing leach solution 45

may be provided to the tank, for example at one end, to flow

perpendicular to the plane of the parallel anodes and cathodes,

and copper can be deposited at the cathode and water

electrolyzed to form oxygen and protons at the anode with

the application of current. As with conventional electrow- 50

inning cells, the rate at which direct current can be passed

through the cell is effectively limited by the rate at which

copper ions can pass from the solution to the cathode

surface. This rate, called the limiting current density, is a

function of factors such as copper concentration, diffusion 55

coefficient of copper, cell configuration, and level of agitation

of the aqueous solution.

The general chemical process for electrowinning of copper

from acid solution is believed to be as follows:

US 6,972,107 B2

15 16

* * * * *

10. The system of claim 8 wherein said leaching means is

suitable for leaching at least a portion of said inlet stream in

an oxidizing environment at a temperature of from about

100° C. to about 250° C. and at pressure of from about 50

to about 750 psi.

11. The system of claim 8 wherein said reacting means is

suitable for reacting at least a portion of said coppercontaining

material stream with at least a portion of said

copper-containing lean electrolyte stream in the presence of

sulfur dioxide, whereby at least a portion of said copper in

said copper-containing lean electrolyte stream precipitates

as copper sulfide onto at least a portion of the coppercontaining

material in said copper-containing material

stream.

5

12. The system of claim 8 wherein said means for

conditioning said product slurry comprises a liquid-solid

separation circuit adapted to separate at least a portion of

said copper-containing solution in said product slurry from

said residue in said product slurry to yield a copper-containing

solution suitable for electrowinning.

13. The system of claim 8 wherein said means for

conditioning said product slurry comprises means for controlling

the copper concentration of said copper-containing

solution whereby the copper concentration of said coppercontaining

solution entering said electrowinning circuit is

maintained at a level of about 40 gramslliter.

14. The system of claim 8 wherein said means for

40 conditioning said product slurry comprises means for blending

at least a portion of said copper-containing solution with

at least a portion of one or more copper-containing streams

to achieve a desired copper concentration in said coppercontaining

solution.

means for recycling at least a portion of said coppercontaining

lean electrolyte stream from said electrowinning

means to said reacting means, and means for

recycling at least a portion of said copper-containing

lean electrolyte stream from said electrowinning means

to said conditioning means.

9. The system of claim 8 further comprising means for

separating at least a portion of said solid copper-bearing

10 precipitate from said acid to yield a concentrated inlet

stream.

2. The system of claim 1 further comprising a liquid-solid

separation circuit, wherein said liquid-solid separation circuit

is adapted to separate at least a portion of said solid

copper-bearing precipitate from said acid to yield a concentrated

pressure leaching feed stream.

3. The system of claim 1 wherein said pressure leaching

vessel is suitable for leaching at least a portion of said

pressure leaching feed stream at a temperature of from about

100° C. to about 250° C. and at a pressure of from about 50

to about 750 psi.

4. The system of claim 1 wherein said reactor is suitable

for reacting at least a portion of a copper-containing feed

stream with at least a portion of a copper-containing lean

electrolyte stream in the presence of sulfur dioxide, whereby

at least a portion of said copper in said copper-containing 15

lean electrolyte stream precipitates as copper sulfide onto at

least a portion of the copper-containing material in said feed

stream.

5. The system of claim 1 wherein said means for conditioning

said product slurry comprises a liquid-solid separa- 20

tion circuit adapted to separate at least a portion of said

copper-containing solution in said product slurry from said

residue in said product slurry to yield a copper-containing

solution suitable for electrowinning.

6. The system of claim 1 wherein said means for condi- 25

tioning said product slurry comprises means for controlling

the copper concentration of said copper-containing solution.

7. The system of claim 1 further comprising means for

recycling at least a portion of said copper-containing lean

electrolyte stream from said electrowinning circuit to said 30

reactor.

8. A system for recovering copper from a copper-containing

material comprising:

means for reacting a copper-containing material stream

with a copper-containing lean electrolyte stream to 35

produce an inlet stream comprising a copper-bearing

precipitate and acid;

means for leaching at least a portion of said inlet stream

to produce a product slurry comprising a copper-containing

solution and a residue;

means for conditioning said product slurry without the use

of solvent extraction techniques to produce a coppercontaining

solution acceptable for electrowinning;

means for electrowinning copper from said copper-containing

solution to produce a cathode copper product; 45

and

style=���gn��x8in;margin-bottom:.0001pt;line-height: normal;mso-pagination:none;mso-layout-grid-align:none;text-autospace:none'>extracting at least one metal value from said product comprises

 

extracting gold from said product.

* * * * *


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